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  Global Journal of Inorganic Chemistry. Volume 1, Issue 1 (2010) pp. 76-82
  Research Article
 
Synthesis, characterization and study of products of the thermal decomposition of Bi[FexCo1-x(CN)6].4H2O (0≤x≤1)
  M.Carolina Navarroa, M. Cristina Lagarriguea, Raúl E. Carboniob, M. Inés Gómeza*  
     
a Instituto de Química Inorgánica. Facultad de Bioquímica, Química y Farmacia. Universidad Nacional de Tucumán. Ayacucho 471. 4000. San Miguel de Tucumán, Argentina
b Departamento de Fisicoquímica. Facultad de Ciencias Químicas. Instituto de Investigaciones en Fisicoquímica de Córdoba (INFIQC). Universidad Nacional de Córdoba. Ciudad Universitaria. 5000. Córdoba, Argentina

   
  Abstract  
  In order to investigate the formation of the solid solution BiFexCo1-xO3, the synthesis and thermal decomposition of the inorganic complex Bi[FexCo1-x(CN)6].4H2O has been studied. The starting material and the decomposition products were characterized by IR spectroscopy, thermal analysis, laboratory powder X-ray diffraction and microscopic electron scanning. The crystal structures of these compounds were refined by Rietveld analysis. BiFexCo1-xO3 were obtained from the thermal decomposition at 600 ºC of the complexes for values of x = 0.7-1.0.
     
  Keywords  
  Bismuth iron oxide; Low temperature synthesis; Multiferroic materials; X-ray diffraction  
     
   
   
   
   
     

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