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  Journal of Nanoscience Letters. Volume 1, Issue 2 (2011) pp. 123-127
  Research Article
Synthesis and electron-transfer properties of cofactor MoFe nanocrystals by one-pot reaction
  Weizhong Sun, Zhengji Zhou, Xia Wang, Wenhui Zhou, Sixin Wu  
Key Laboratory for Special Functional Materials of Minnistry of Education, Henan University, Kaifeng 475004, China
  The cofactor MoFe nanocrystals were synthesized based on pyrolysis by one-pot in oleyamine for the first time. The images of transmission electron microscopy demonstrated the as-prepared cofactor MoFe were composed of monodispersed, uniform nanocrystals with diameters of about 2~4 nm. The composition of the as-prepared cofactor MoFe nanocrystals was confirmed as MoFe6S8 by X-ray Diffraction, Energy-Dispersive spectra and X-ray Photoelectron Spectroscopy. Unlike the previous anaerobic MoFeco clusters, the as-prepared cofactor MoFe nanocrystals are not sensitive to oxygen. The electron-transfer performance of cofactor MoFe nanocrystals was conducted through electrochemical measurement at ambient atmosphere. The result of cyclic voltammograms illuminated that the cofactor MoFe nanocrystals displays successive reversible electron- transfer process.
  MoFeS; Nanocrystal; Synthesis; Electron-transfer  

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